Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,4-Dichlorocinnamic acid → (R)-1-[(E)-3-(3,4-Dichloro-phenyl)-acryloyl]-2-methyl-[1,4]diazepan-5-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,4-Dichlorocinnamic acid | HCID 688027 | — |
| 반응물 | (R)-2-methyl-[1,4]diazepan-5-one | HCID 28064214 | — |
| 생성물 | (R)-1-[(E)-3-(3,4-Dichloro-phenyl)-acryloyl]-2-methyl-[1,4]diazepan-5-one | HCID 68432228 | — |
반응 단계
In analogy to the procedure described in intermediate 78C, (E)-3,4-dichlorocinnamic acid and (R)-2-methyl-[1,4]diazepan-5-one gave the title compound as a colorless gum, MS: m/e=327.3 (MH+).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07632829B2 |
| 출처 데이터셋 | uspto-grants-2009_12 |
| ORD ID | ord-8141f72d1a7e473faea850fcd678cc96 |
| 출처 메모 | uspto-grants-2009_12 |