5-Bromo-2,1,3-benzoxadiazole → HCID 86604698, 화합물

반응식

Br[C:2]1[CH:3]=[CH:4][C:5]2[C:6]([CH:10]=1)=[N:7][O:8][N:9]=2.C(OC(=O)[N:17]([C:21]1[CH:26]=[CH:25][C:24](Br)=[C:23]([O:28][CH3:29])[CH:22]=1)[CH2:18][CH2:19][F:20])(C)(C)C>>[N:9]1[O:8][N:7]=[C:6]2[CH:10]=[C:2]([C:24]3[CH:25]=[CH:26][C:21]([NH:17][CH2:18][CH2:19][F:20])=[CH:22][C:23]=3[O:28][CH3:29])[CH:3]=[CH:4][C:5]=12

참가 물질

반응물 2

HCID 27762985-Bromo-2,1,3-benzoxadiazole

HCID 86604699HCID 86604699, 화합물

생성물 1

HCID 86604698HCID 86604698, 화합물

실험 절차

The starting compound is obtained according to the procedure described in Example 7 from 5-bromo-benzo[1,2,5]oxadiazole and (4-bromo-3-methoxy-phenyl)-(2-fluoro-ethyl)-carbamic acid tert-butyl ester, as a yellow glass. MS(ES+): 410 (M+23).

후처리

customThe starting compound is obtained

출처 및 근거

ORD 기록: ord-12448b13795247ea8d8609fcddc00345
출처 데이터셋: uspto-grants-2009_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07632851B2

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