Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → gamma-Tocotrienol acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | Gamma-Tocotrienol | HCID 5282349 | — |
| 용매 | Ethylacetate heptane | HCID 21899848 | — |
| 생성물 | gamma-Tocotrienol acetate | HCID 86755580 | — |
반응 단계
γ-Tocotrienol (crude product, prepared in accordance with Example 3, 4.8 g) was heated with 10 ml of acetic anhydride for 3.5 h under reflux and then freed from acetic acid and acetic anhydride under reduced pressure. Flash chromatography of the crude product with ethyl acetate/heptane as eluent on silica gel gave 3.7 g of γ-tocotrienol acetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06096907 |
| 출처 데이터셋 | uspto-grants-2000_08 |
| ORD ID | ord-261713b2aa0748a5a4ec098f58ccb7a6 |
| 출처 메모 | uspto-grants-2000_08 |