Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methoxybenzyl chloride → 4,5-Dihydro-2-[2-[2-[3-Methoxyphenyl]ethyl]-4-methylphenyl]-4,4-dimethyloxazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methoxybenzyl chloride | HCID 69994 | — |
| 반응물 | 2-[2,4-Dimethylphenyl]-4,5-dihydro-4,4-dimethyloxazole | HCID 22117273 | — |
| 생성물 | 4,5-Dihydro-2-[2-[2-[3-Methoxyphenyl]ethyl]-4-methylphenyl]-4,4-dimethyloxazole | HCID 18689703 | — |
반응 단계
The subtitle compound was prepared from the product of example 15 step (iii) (20 g) and 3-methoxybenzyl chloride (17.4 ml) by the method of example 15 step (iv). Purification was by chromatography eluting with 5-10% ethyl acetate in isohexane. Yield 20.53 g. MS: APCI(+ve): 324 (M+1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06107297 |
| 출처 데이터셋 | uspto-grants-2000_08 |
| ORD ID | ord-bc4350c96f7f451a94aa710a435535ca |
| 출처 메모 | uspto-grants-2000_08 |