Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tert-butyl 3-(6-nitropyridin-3-yloxy)phenylcarbamate → Tert-butyl 3-(6-aminopyridin-3-yloxy)phenylcarbamate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tert-butyl 3-(6-nitropyridin-3-yloxy)phenylcarbamate | HCID 57749209 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | Tert-butyl 3-(6-aminopyridin-3-yloxy)phenylcarbamate | HCID 57749334 | 106.6% |
반응 단계
In the same manner as in Reference Example 34 and using tert-butyl {3-[(6-nitropyridin-3-yl)oxy]phenyl}carbamate (16.4 g, 49.5 mmol), palladium carbon (50% water-containing product, 1.50 g) and methanol (100 mL) as starting materials, the title compound (15.9 g, quant.) was obtained as a yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08304557B2 |
| 출처 데이터셋 | uspto-grants-2012_11 |
| ORD ID | ord-a02cc20b73f54b1aa2c9721bf3bc5b73 |
| 출처 메모 | uspto-grants-2012_11 |