Thionyl Chloride → HCID 23144827, 화합물

HRID 1875554노트

반응식

Cl.[CH3:2][N:3]([CH2:5][C:6]1[C:7]([N+:15]([O-:17])=[O:16])=[C:8]([CH:12]=[CH:13][CH:14]=1)[C:9](O)=[O:10])[CH3:4].S(Cl)([Cl:20])=O>>[CH3:2][N:3]([CH2:5][C:6]1[C:7]([N+:15]([O-:17])=[O:16])=[C:8]([CH:12]=[CH:13][CH:14]=1)[C:9]([Cl:20])=[O:10])[CH3:4]

참가 물질

반응물 2

HCID 24386Thionyl Chloride

HCID 69203826HCID 69203826, 화합물

생성물 1

HCID 23144827HCID 23144827, 화합물

반응 조건

온도: 80 °C

실험 절차

The mixture of 3-dimethylaminomethyl-2-nitrobenzoic acid hydrochloride (0.1 g) and thionylchloride (5 mL) was stirred at 80° C. for 3 hours. The solvent was removed and the residue was dried to obtain 3-dimethylamino methyl-2-nitrobenzoyl chloride.

후처리

customThe solvent was removed
customthe residue was dried

출처 및 근거

ORD 기록: ord-dbbba8b3f9234078905a6bdb7e95cc15
출처 데이터셋: uspto-grants-2012_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08309561B2

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