Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-(2,4-Difluorophenyl)-2-methyl-3-furaldehyde → Cyclohexyl[5-(2,4-difluorophenyl)-2-methyl-3-furyl]methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-(2,4-Difluorophenyl)-2-methyl-3-furaldehyde | HCID 83595645 | — |
| 반응물 | HCID 178420632 | HCID 178420632 | — |
| 생성물 | Cyclohexyl[5-(2,4-difluorophenyl)-2-methyl-3-furyl]methanol | HCID 68515112 | 76% |
반응 단계
An operation similar to that in Example 3 (2) was performed using 5-(2,4-difluorophenyl)-2-methyl-3-furaldehyde (2.4 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (16.5 mL) to give the title compound (2.6 g, 76%) as a white crystal.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08309580B2 |
| 출처 데이터셋 | uspto-grants-2012_11 |
| ORD ID | ord-11bb2b91221f40989159f4c2f696dd35 |
| 출처 메모 | uspto-grants-2012_11 |