Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-(4-Chloro-2-methylphenyl)-2-methyl-3-furaldehyde → [5-(4-Chloro-2-methylphenyl)-2-methyl-3-furyl] (cyclohexyl)methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-(4-Chloro-2-methylphenyl)-2-methyl-3-furaldehyde | HCID 86646368 | — |
| 용매 | HCID 178420632 | HCID 178420632 | — |
| 생성물 | [5-(4-Chloro-2-methylphenyl)-2-methyl-3-furyl] (cyclohexyl)methanol | HCID 68514219 | 156.4% |
반응 단계
An operation similar to that in Example 3 (2) was performed using 5-(4-chloro-2-methylphenyl)-2-methyl-3-furaldehyde (1.6 g) and 1N cyclohexylmagnesium bromide-tetrahydrofuran solution (10 mL) to give the title compound (1.7 g, 77%) as a white crystal.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08309580B2 |
| 출처 데이터셋 | uspto-grants-2012_11 |
| ORD ID | ord-190b2a545df64902b5ffe700b3d0a12f |
| 출처 메모 | uspto-grants-2012_11 |