Thionyl Chloride → HCID 68515497, 화합물

HRID 1877062노트

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HRID 1877062 반응식
[CH3:1][CH:2]([CH3:18])[CH2:3][CH:4]([C:6]1[CH:10]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[O:8][C:7]=1[CH3:17])O.S(Cl)([Cl:21])=O>C1(C)C=CC=CC=1>[Cl:21][CH:4]([C:6]1[CH:10]=[C:9]([C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=2)[O:8][C:7]=1[CH3:17])[CH2:3][CH:2]([CH3:18])[CH3:1]

참가 물질

4

반응물 2

HCID 24386Thionyl ChlorideHCID 685095783-Methyl-1-(2-methyl-5-phenylfuran-3-yl)butan-1-ol

생성물 1

HCID 68515497HCID 68515497, 화합물수율 100%

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

To a solution of 3-methyl-1-(2-methyl-5-phenylfuran-3-yl)butan-1-ol (1.5 g) in toluene (20 mL) was added thionyl chloride (0.9 mL), and the mixture was stirred at room temperature overnight. The solvent was evaporated under reduced pressure to give the title compound (1.6 g, 100%) as an oil.

후처리

  1. customThe solvent was evaporated under reduced pressure

출처 및 근거

ORD 기록
ord-059cce386ae5449980b3c2710eff9d05
출처 데이터셋
uspto-grants-2012_11
특허 번호
US08309580B2

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