Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3,3'-Dibenzyloxybiphenyl → 3,3'-Biphenyldiol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3,3'-Dibenzyloxybiphenyl | HCID 66671258 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 3,3'-Biphenyldiol | HCID 69165 | — |
반응 단계
146 g (0.392 mol) of 3,3′-dibenzyloxybiphenyl are dissolved in 1.5 I of THF and hydrogenated to completion on a Pd/C catalyst. The catalyst is filtered off, the filtrate is evaporated, and the residue is filtered through silica gel with toluene/ethyl acetate, giving biphenyl-3,3′-diol as a colourless solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08313669B2 |
| 출처 데이터셋 | uspto-grants-2012_11 |
| ORD ID | ord-ce95411915da491dae99ad885ce04eb6 |
| 출처 메모 | uspto-grants-2012_11 |