Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,4-Difluorobenzoic acid → 1-Methyl-4-nitrosopiperidin-4-yl 2,4-difluorobenzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,4-Difluorobenzoic acid | HCID 74102 | — |
| 반응물 | 1-Methylpiperidin-4-one oxime | HCID 339053 | — |
| 반응물 | HCID 178418268 | HCID 178418268 | — |
| 생성물 | 1-Methyl-4-nitrosopiperidin-4-yl 2,4-difluorobenzoate | HCID 57954497 | — |
반응 단계
1-Methyl-4-nitrosopiperidin-4-yl 2,4-difluorobenzoate was prepared from 1-methyl-piperidin-4-one oxime, lead tetraacetate and 2,4-difluorobenzoic acid using conditions of General Method 3. 1H NMR (400 MHz, chloroform-d) δ 7.59 (2H, dd, 7.5, 2.3 Hz), 7.09 (1H, tt, 8.6, 2.4 Hz), 2.98 (2H, dt, 11.7, 3.6 Hz), 2.32-2.50 (7H, m), 2.04 (2H, dd, 14.2, 2.7 Hz).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08318705B2 |
| 출처 데이터셋 | uspto-grants-2012_11 |
| ORD ID | ord-1eed22c0b45144449688068e39867685 |
| 출처 메모 | uspto-grants-2012_11 |