Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chlorodifluoroacetic acid → 4-Nitrosotetrahydro-2H-pyran-4-yl 2-chloro-2,2-difluoroacetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chlorodifluoroacetic acid | HCID 66154 | — |
| 반응물 | N-(oxan-4-ylidene)hydroxylamine | HCID 12298558 | — |
| 반응물 | HCID 178418268 | HCID 178418268 | — |
| 생성물 | 4-Nitrosotetrahydro-2H-pyran-4-yl 2-chloro-2,2-difluoroacetate | HCID 44479142 | — |
반응 단계
4-Nitrosotetrahydro-2H-pyran-4-yl 2-chloro-2,2-difluoroacetate was prepared from tetrahydro-pyran-4-one oxime, lead tetraacetate and chlorodifluoroacetic acid using conditions of General Method 3. 1H NMR (360 MHz, chloroform-d) δ 4.06-4.23 (2H, m), 3.52-3.86 (2H, m), 2.27-2.70 (2H, m), 1.72-2.07 (2H, m).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08318705B2 |
| 출처 데이터셋 | uspto-grants-2012_11 |
| ORD ID | ord-7a6c5527225440c28a5f2f59810a2bd2 |
| 출처 메모 | uspto-grants-2012_11 |