Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Pivalic acid → 1,2,2,6,6-Pentamethyl-4-nitrosopiperidin-4-yl pivalate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Pivalic acid | HCID 6417 | — |
| 반응물 | 1,2,2,6,6-Pentamethyl-piperidin-4-one oxime | HCID 241950 | — |
| 반응물 | HCID 178418268 | HCID 178418268 | — |
| 생성물 | 1,2,2,6,6-Pentamethyl-4-nitrosopiperidin-4-yl pivalate | HCID 57954471 | — |
반응 단계
1,2,2,6,6-Pentamethyl-4-nitrosopiperidin-4-yl pivalate was prepared from 1,2,2,6,6-pentamethyl-piperidin-4-one oxime, lead tetraacetate and trimethylacetic acid using conditions of General Method 3. 1H NMR (250 MHz, CHLOROFORM-d) δ 2.43-2.64 (5H, m), 2.09 (3H, s), 1.91 (2H, d, 14.2 Hz), 1.39 (6H, d, 5.9 Hz), 1.30 (9H, s), 1.25 (6H, d, 2.6 Hz).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08318705B2 |
| 출처 데이터셋 | uspto-grants-2012_11 |
| ORD ID | ord-c47e4a33ebf44f39b0ce4364c49f4b18 |
| 출처 메모 | uspto-grants-2012_11 |