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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1880141생성일: 2026년 10월 25일

HCID 59327113, 화합물 → Tert-butyl 4-(2-(4-(ethoxycarbonyl)phenoxy)pyridin-3-YL)piperidine-1-carboxylate

https://huagongshe.com/reaction/1880141

반응식

참여 물질

역할이름HCID투입량
반응물HCID 59327113HCID 59327113—
촉매Palladium hydroxideHCID 9942167—
용매EthanolHCID 702—
생성물Tert-butyl 4-(2-(4-(ethoxycarbonyl)phenoxy)pyridin-3-YL)piperidine-1-carboxylateHCID 59326865—

반응 단계

A mixture of tert-butyl 4-(2-(4-(ethoxycarbonyl)phenoxy)pyridin-3-yl)-5,6-dihydropyridine-1(2H)-carboxylate (5.89 g, 13.87 mmol) and palladium hydroxide on carbon (0.950 g, 1.353 mmol) in EtOH (50 mL) was evacuated/purged with hydrogen (1 atm, 3×). After stirring at rt overnight. The mixture was filtered through a pad of Celite and the filtrate was concentrated to dryness to give a light-yellow oil. MS m/z: 427.1 [M+1].

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08318718B2
출처 데이터셋uspto-grants-2012_11
ORD IDord-f247155a94ad4058a61b4bf159cec40a
출처 메모uspto-grants-2012_11