Nitric Acid → HCID 86633440, 화합물
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[CH2:1]([O:3][C:4]1[C:5]([OH:15])=[CH:6][C:7]([N+:12]([O-:14])=[O:13])=[C:8]([CH:11]=1)[CH:9]=[O:10])[CH3:2].[N+:16]([O-])([OH:18])=[O:17]>ClCCl>[CH2:1]([O:3][C:4]1[C:5]([OH:15])=[C:6]([N+:16]([O-:18])=[O:17])[C:7]([N+:12]([O-:14])=[O:13])=[C:8]([CH:11]=1)[CH:9]=[O:10])[CH3:2]참가 물질
4
실험 절차
5-Ethoxy-4-hydroxy-2-nitro-benzaldehyde (1.6 g) was dissolved in dichloromethane (30 ml) and a solution of nitric acid in dichloromethane (2M, 13 ml) was gradually added at a temperature under 30° C. The solution was stirred at room temperature for 10 min and then it was poured into ice-cold water. The organic phase was washed with water and then it was dried and evaporated.
후처리
- additionit was poured into ice-cold water
- washThe organic phase was washed with water
- customit was dried
- customevaporated
출처 및 근거
- ORD 기록
- ord-54c530f1a88d424cae06118e9b210021
- 출처 데이터셋
- uspto-grants-2012_11
- 특허 번호
- US08318785B2
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