Dimethylformamide → HCID 67094308, 화합물
반응식
[CH2:1]([O:3][C:4]1[C:11]([O:12][CH2:13][CH3:14])=[CH:10][C:7]([CH:8]=O)=[C:6]([N+]([O-])=O)[C:5]=1[N+:18]([O-:20])=[O:19])[CH3:2].[CH3:21]N(C)C=O.C[CH:27]([SH:31])[C:28]([O-:30])=[O:29]>C(N(CC)CC)C>[CH3:21][O:30][C:28]([C:27]1[S:31][C:6]2[C:5]([N+:18]([O-:20])=[O:19])=[C:4]([O:3][CH2:1][CH3:2])[C:11]([O:12][CH2:13][CH3:14])=[CH:10][C:7]=2[CH:8]=1)=[O:29]참가 물질
5
실험 절차
4,5-Diethoxy-2,3-dinitro-benzaldehyde (1.53 g) was dissolved into N,N-dimethylformamide (6 ml) and then methylthioglycolate (1.36 ml) was added. Triethylamine (2.6 ml) was added in cold to the reaction solution. The mixture was stirred overnight. The solid was filtered and washed with N,N-dimethylformamide.
후처리
- filtrationThe solid was filtered
- washwashed with N,N-dimethylformamide
출처 및 근거
- ORD 기록
- ord-091b2d51415b43bf900a177f8eefff47
- 출처 데이터셋
- uspto-grants-2012_11
- 특허 번호
- US08318785B2
반응 노트
불러오는 중…