Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → (+/-)-Abscisic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | Abscisic Acid | HCID 5280896 | — |
| 반응물 | Potassium Sorbate | HCID 23676745 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | (+/-)-Abscisic acid | HCID 5375199 | — |
반응 단계
(S)-(+)-Abscisic acid (2.64 g of 95% purity) was suspended in 15 mL of deionized water containing 50 mg of Tween 20. One quarter of the theoretical amount of potassium hydroxide (250 microL of 10.0 molar aqueous solution) was added. The remainder of the neutralization was then carried out with concentrated aqueous ammonia solution, to give a clear solution of pH 7.1. Preservative (63 mg of potassium sorbate) was added, and it quickly dissolved. The solution was made up to 25 mL final volume to give a 10% by weight aqueous composition of abscisic acid as a mixture of the ammonium and potassium salts.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08318976B2 |
| 출처 데이터셋 | uspto-grants-2012_11 |
| ORD ID | ord-f2fd709f55464c6193b3cb8ac0b56f91 |
| 출처 메모 | uspto-grants-2012_11 |