3-Bromobenzene-1-sulfonamide → 3-(4,4-Dimethyl-2-oxo-1,4-dihydro-2H-benzo[d][1,3]-oxazin-6-yl)benzenesulfonamide

참여 물질

역할	이름	HCID	투입량
반응물	3-Bromobenzene-1-sulfonamide	HCID 2734765	—
반응물	(4,4-Dimethyl-2-oxo-1,4-dihydro-2H-3,1-benzoxazin-6-yl)boronic acid	HCID 10987806	—
생성물	3-(4,4-Dimethyl-2-oxo-1,4-dihydro-2H-benzo[d][1,3]-oxazin-6-yl)benzenesulfonamide	HCID 12094506	—

반응 단계

Prepared according to procedure B from 3-bromobenzenesulfonamide and (1,4-dihydro-4,4-dimethyl-2-oxo-2H-3,1-benzoxazin-6-yl)boronic acid. White solid: mp 242-244° C. (dec) 1H-NMR (DMSO-d6) δ10.28 (s, broad 1H), 8.07 (s, 1H), 7.9 (d, 1H, J=7.80 Hz), 7.78 (d, 1H, J=7.86 Hz), 7.64 (t, 1H, J=7.79 Hz), 7,59 (m, 2H), 7.42 s, broad 2H), 7.02 (d, 1H, J=8.86 Hz), 1.68 (s, 6H); MS m/z 331(M+H). Anal. Calc. For C16H16N2O4S: C, 57.82; H, 4.85; N, 8.43. Found: C, 57.49; H, 5.08; N, 8.05.

출처 및 근거

DOI	10.6084/m9.figshare.5104873.v1
특허 번호	US06759408B2
출처 데이터셋	uspto-grants-2004_07
ORD ID	ord-df60d7a0155d4f3bb205b972264958fd
출처 메모	uspto-grants-2004_07