2-Amino-3-bromobenzaldehyde → (2-Amino-3-bromophenyl)methanol

반응식

NC1C(C=O)=CC=CC=1C(OC)=O.[NH2:14][C:15]1[C:22]([Br:23])=[CH:21][CH:20]=[CH:19][C:16]=1[CH:17]=[O:18]>>[NH2:14][C:15]1[C:22]([Br:23])=[CH:21][CH:20]=[CH:19][C:16]=1[CH2:17][OH:18]

참가 물질

반응물 2

HCID 100814842-Amino-3-bromobenzaldehyde

HCID 10773683Methyl 2-amino-3-formylbenzoate

생성물 1

HCID 23510439(2-Amino-3-bromophenyl)methanol

실험 절차

In a similar manner to the preparation of methyl 2-amino-3-formylbenzoate, 2-amino-3-bromobenzaldehyde (3.28 g, quantitatively) was obtained from (2-amino-3-bromophenyl)methanol (3.27 g).

출처 및 근거

ORD 기록: ord-1aa32c7f8189425891fda1d732f1c970
출처 데이터셋: uspto-grants-2004_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06759429B2

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