Silver Nitrate → Acesulfame silver

HRID 1883215

반응식

HRID 1883215 반응식
[N+]([O-])([O-])=O.[Ag+:5].[CH3:6][C:7]1[O:15][S:12](=[O:14])(=[O:13])[N-:11][C:9](=[O:10])[CH:8]=1.[K+]>O>[CH3:6][C:7]1[O:15][S:12](=[O:14])(=[O:13])[NH:11][C:9](=[O:10])[CH:8]=1.[Ag:5]

참가 물질

4

반응물 2

HCID 24470Silver NitrateHCID 11074431Acesulfame Potassium

생성물 1

HCID 131724477Acesulfame silver수율 88%

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

A solution of 30 mmol (5.148 g) of silver(I) nitrate in 30 ml of water was added to a solution of 30 mmol (6.037 g) of acesulfame-K in 30 ml of water. After addition was complete, the colorless precipitate formed was filtered off by suction and washed twice, each time with 10 ml of water. 88% of colorless acesulfame-silver crystals resulted. The reaction and subsequent workup as described above need not be carried out in the absence of light.

후처리

  1. additionAfter addition
  2. customthe colorless precipitate formed
  3. filtrationwas filtered off by suction
  4. washwashed twice

출처 및 근거

ORD 기록
ord-a719c7edd0914d6fa57be7d45727584e
출처 데이터셋
uspto-grants-2004_07
특허 번호
US06759544B2

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