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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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HCID 69859806, 화합물 → HCID 23508311, 화합물

HRID 1883714
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HRID 1883714 반응식
[C:1]([NH:4][C:5]1[CH:6]=[CH:7][C:8]([C:14]([CH3:21])=[CH:15][C:16]([O:18][CH2:19][CH3:20])=[O:17])=[C:9]2[C:13]=1[CH2:12][CH2:11][CH2:10]2)(=[O:3])[CH3:2]>C(O)C.[Pd]>[C:1]([NH:4][C:5]1[CH:6]=[CH:7][C:8]([CH:14]([CH3:21])[CH2:15][C:16]([O:18][CH2:19][CH3:20])=[O:17])=[C:9]2[C:13]=1[CH2:12][CH2:11][CH2:10]2)(=[O:3])[CH3:2]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 1

HCID 69859806HCID 69859806, 화합물

생성물 1

HCID 23508311HCID 23508311, 화합물수율 86.8%

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 702Ethanol용매

실험 절차

A solution of ethyl 3-[7-acetylamino-indan-4-yl]-but-2-enoate (1.9 g, Reference Example 7) in ethanol (200 mL) was hydrogenated over 10% palladium on charcoal for 16 hours. The mixture was filtered through diatomaceous earth and the filtrate was evaporated to give the title compound (1.66 g).

후처리

  1. filtrationThe mixture was filtered through diatomaceous earth
  2. customthe filtrate was evaporated

출처 및 근거

ORD 기록
ord-434ee3510dec4a728e8def25a85bbf26
출처 데이터셋
uspto-grants-2004_07
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06762199B2

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