4-Bromobenzaldehyde → E-4-bromostyryl 4-fluorobenzyl sulfone

HRID 1885001노트

반응식

HRID 1885001 반응식
[F:1][C:2]1[CH:15]=[CH:14][C:5]([CH2:6][S:7]([CH2:10][C:11](O)=O)(=[O:9])=[O:8])=[CH:4][CH:3]=1.[Br:16][C:17]1[CH:24]=[CH:23][C:20](C=O)=[CH:19][CH:18]=1>>[F:1][C:2]1[CH:15]=[CH:14][C:5]([CH2:6][S:7](/[CH:10]=[CH:11]/[C:20]2[CH:23]=[CH:24][C:17]([Br:16])=[CH:18][CH:19]=2)(=[O:9])=[O:8])=[CH:4][CH:3]=1

참가 물질

3

반응물 2

HCID 707414-BromobenzaldehydeHCID 11447598[(4-Fluorobenzyl)sulfonyl]acetic acid

생성물 1

HCID 9798714E-4-bromostyryl 4-fluorobenzyl sulfone수율 82%

실험 절차

A solution of 4-fluorobenzyl sulfonylacetic acid (0.01 mol) and 4-bromobenzaldehyde (0.01 mol) was subjected to Procedure 1, Part B. The title compound was obtained in 82% yield.

출처 및 근거

ORD 기록
ord-5a98a1d12c5b41629caf5aa64e008575
출처 데이터셋
uspto-grants-2004_07
특허 번호
US06767926B1

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