반응식
[OH:1][C:2]1[CH:7]=[C:6]([OH:8])[CH:5]=[CH:4][C:3]=1[C:9](=O)[CH2:10][CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.[NH2:20][C:21]1[CH:26]=[CH:25][C:24]([C:27]2[CH2:28][CH2:29][C:30](=[O:33])[NH:31][N:32]=2)=[CH:23][CH:22]=1>C(OCC)(=O)C>[OH:1][C:2]1[CH:7]=[C:6]([OH:8])[CH:5]=[CH:4][C:3]=1[C:9](=[N:20][C:21]1[CH:26]=[CH:25][C:24]([C:27]2[CH2:28][CH2:29][C:30](=[O:33])[NH:31][N:32]=2)=[CH:23][CH:22]=1)[CH2:10][CH2:11][CH2:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1참가 물질
4
반응 조건
- 온도
- 150 °C
실험 절차
A mixture containing 0.2 g of 1-(2,4-dihydroxyphenyl)4-phenylbutan-1-one and 6-(4-aminophenyl)-4,5-dihydropyridazin-3(2H)one was heated for 24 h at 150° C. The product was treated with ethyl acetate. Yield 0.2 g (88%), m.p. 274°-280° C.
출처 및 근거
- ORD 기록
- ord-a67c1bcb683b401ca5c3a127faa5cfa5
- 출처 데이터셋
- uspto-grants-1992_09
- 특허 번호
- US05151420
연결된 노트
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