Ammonia → HCID 53938285, 화합물

HRID 1886331노트

반응식

HRID 1886331 반응식
C([O:3][C:4]([C@@H:6]([NH:10][C@H:11]([C:13]([OH:15])=[O:14])[CH3:12])[CH2:7][CH2:8][CH3:9])=O)C.[NH3:16]>>[C:4]([C@@H:6]([NH:10][C@H:11]([C:13]([OH:15])=[O:14])[CH3:12])[CH2:7][CH2:8][CH3:9])(=[O:3])[NH2:16]

참가 물질

3

반응물 2

HCID 222AmmoniaHCID 10015159(2S)-2-[[(2S)-1-ethoxy-1-oxopentan-2-yl]amino]propanoic acid

생성물 1

HCID 53938285HCID 53938285, 화합물수율 95%

실험 절차

10 g of (S)-N-[(S)-1-(ethoxycarbonyl)butyl]alanine are placed in 100 ml of 28% strength aqueous ammonia solution at 100° C. for 18 hours. After evaporation of the solvent, the residue is taken up with 50 ml of water. The solution is evaporated to dryness, then taken up with 100 ml of isopropanol and evaporated. The expected product is obtained after drying under vacuum.

후처리

  1. customAfter evaporation of the solvent
  2. customThe solution is evaporated to dryness
  3. customevaporated

출처 및 근거

ORD 기록
ord-b1e93e124c40401ea4ff2b26d93c20a7
출처 데이터셋
uspto-grants-1992_09
특허 번호
US05151432

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