Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-5-chlorobenzophenone → N-(2-benzoyl-4-chlorophenyl)-4-tert-butylbenzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-5-chlorobenzophenone | HCID 12870 | — |
| 반응물 | 4-t-Butylbenzenesulfonyl chloride | HCID 139882 | — |
| 생성물 | N-(2-benzoyl-4-chlorophenyl)-4-tert-butylbenzenesulfonamide | HCID 1732024 | — |
반응 단계
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 115 mg of (2-amino-5-chloro-phenyl)-phenyl-methanone and 116 mg of 4-tert-Butyl-benzenesulfonyl chloride. 1H-NMR (400 MHz, CDCl3): δ 1.21 (s, 9H), 7.28-7.34 (m, 3H), 7.37-7.44 (m, 4H), 7.48 (dd, 1H, J=8.8, 2.4 Hz), 7.54-7.62 (m, 3H), 7.78 (d, 1H, J=8.8 Hz), 9.89 (s, 1H). MS: m/z 428.9 (M++1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741519B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-374695e114374437a6695199ecac9f38 |
| 출처 메모 | uspto-grants-2010_06 |