Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-5-chlorobenzophenone → N-(2-benzoyl-4-chloro-phenyl)-2,4-dichloro-benzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-5-chlorobenzophenone | HCID 12870 | — |
| 반응물 | Benzenesulfonyl chloride, 2,4-dichloro- | HCID 204419 | — |
| 생성물 | N-(2-benzoyl-4-chloro-phenyl)-2,4-dichloro-benzenesulfonamide | HCID 11247683 | — |
반응 단계
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 115 mg of (2-amino-5-chloro-phenyl)-phenyl-methanone and 123 mg of 2,4-dichloro-benzenesulfonyl chloride. 1H-NMR (400 MHz, CDCl3): δ 7.24 (m, 1H), 7.31 (m, 1H), 7.45 (m, 2H), 7.54 (m, 2H), 7.60-7.65 (m, 2H), 7.97 (d, 1H, J=8.4 Hz), 10.23 (s, 1H). MS: m/z 440.7 (M++1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741519B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-c371b57b7eb2404e8edfb0b27e2bf8ac |
| 출처 메모 | uspto-grants-2010_06 |