Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-5-bromobenzophenone → N-(2-benzoyl-4-bromo-phenyl)-4-ethyl-benzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-5-bromobenzophenone | HCID 99677 | — |
| 반응물 | 4-Ethylbenzene-1-sulfonyl chloride | HCID 570959 | — |
| 생성물 | N-(2-benzoyl-4-bromo-phenyl)-4-ethyl-benzenesulfonamide | HCID 10456110 | — |
반응 단계
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 138 mg of (2-amino-5-bromo-phenyl)-phenyl-methanone and 102 mg of 4-Ethyl-benzenesulfonyl chloride. 1H-NMR (400 MHz, CDCl3): δ 1.13 (t, 3H, J=7.6 Hz), 2.54 (q, 2H, 14.8 Hz, 7.6 Hz), 7.08 (d, 2H, J=8.8 Hz), 7.35-7.43 (m, 4H), 7.46 (d, 1H, J=2.4 Hz), 7.55-7.63 (m, 4H), 7.69 (d, 1H, J=8.8 Hz), 9.78 (s, 1H). m/z 445.3 (M++1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741519B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-04454dead0b74f0b8ffa2c94b699c69e |
| 출처 메모 | uspto-grants-2010_06 |