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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1888270생성일: 2026년 10월 26일

Triethylamine → HCID 178477702, 화합물

https://huagongshe.com/reaction/1888270

반응식

참여 물질

역할이름HCID투입량
반응물TriethylamineHCID 8471—
반응물Ethanesulfonyl chlorideHCID 11667—
반응물HCID 178479542HCID 178479542—
용매DichloromethaneHCID 6344—
생성물HCID 178477702HCID 178477702—

반응 단계

This compound was prepared in a fashion analogous to the procedure described in Example 3. Thus, 3-(4-piperidinyl)-5-(3-thienyl)-1H-indazole-7-carboxamide hydrochloride (Intermediate 19) (0.117 mmol) was reacted with ethane sulfonyl chloride (0.02 mL, 0.234 mmol) in the presence of triethylamine (0.04 mL, 0.468 mmol) in methylene chloride (10 mL) to give the title compound (9.4 mg, 19% for the last two steps)

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08501780B2
출처 데이터셋uspto-grants-2013_08
ORD IDord-8d288bc1b3644834885618bae5388d28
출처 메모uspto-grants-2013_08