Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-Acetylsulfanilyl chloride → N-[4-(2-Benzoyl-4-chloro-phenylsulfamoyl)-phenyl]-acetamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-Acetylsulfanilyl chloride | HCID 8481 | — |
| 반응물 | 2-Amino-5-chlorobenzophenone | HCID 12870 | — |
| 생성물 | N-[4-(2-Benzoyl-4-chloro-phenylsulfamoyl)-phenyl]-acetamide | HCID 3481101 | — |
반응 단계
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 115 mg of (2-amino-5-chloro-phenyl)-phenyl-methanone and 117 mg of 4-Acetylamino-benzenesulfonyl chloride. 1H-NMR (400 MHz, CDCl3): δ 2.16 (s, 3H), 7.26 (b, 1H), 7.33 (d, 1H, J=2.4 Hz), 7.39 (m, 6H), 7.46 (dd, 1H, J=8.4 Hz, 2.4 Hz), 7.55 (m, 3H), 7.71 (d, 1H, J=8.8 Hz), 9.74 (s, 1H). MS: m/z 429.0 (M++1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741519B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-b3da01bb68d94b3588fcb7911db29b30 |
| 출처 메모 | uspto-grants-2010_06 |