Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Amino-5-chlorobenzophenone → N-(2-Benzoyl4-chloro-phenyl)4-trifluoromethoxy-benzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Amino-5-chlorobenzophenone | HCID 12870 | — |
| 반응물 | p-(Trifluoromethoxy)benzenesulphonyl chloride | HCID 523102 | — |
| 생성물 | N-(2-Benzoyl4-chloro-phenyl)4-trifluoromethoxy-benzenesulfonamide | HCID 10321805 | — |
반응 단계
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using (2-amino-5-chloro-phenyl)-phenyl-methanone and 4-Trifluoromethoxy-benzenesulfonyl chloride. 1H NMR (CDCl3): δ 7.06 (d, J=8.0 Hz, 2H), 7.36 (m, 3H), 7.40-7.44 (m, 2H), 7.49 & 7.62 (dd, J=8.8 Hz, 2.0 Hz, 1H), 7.58-7.62 (m, 1H), 7.70 (d, J=8.8 Hz, 2H), 7.70 (d, J=8.8 Hz, 1H), 9.81 (s, 1H). MS: m/z 456.0 (M++1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07741519B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-8062ece2cfc94a04b0d411ae947f3109 |
| 출처 메모 | uspto-grants-2010_06 |