Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Hydroxy-2-naphthoic acid → 4-Bromo-1-hydroxynaphthalene-2-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Hydroxy-2-naphthoic acid | HCID 6844 | — |
| 반응물 | Bromine | HCID 24408 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 4-Bromo-1-hydroxynaphthalene-2-carboxylic acid | HCID 289393 | — |
반응 단계
To a solution of 2.50 g 1-hydroxy-2-naphthoic acid in 50 ml chloroform a solution of 0.68 ml bromine in 5 ml chloroform was added dropwise. After 16 h the reaction was concentrated to yield 3.40 g 4-bromo-1-hydroxy-naphthalene-2-carboxylic acid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08501981B2 |
| 출처 데이터셋 | uspto-grants-2013_08 |
| ORD ID | ord-c476824724194ed09ca48b85851eeef4 |
| 출처 메모 | uspto-grants-2013_08 |