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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1890704생성일: 2026년 10월 27일

Triethylamine → N-[1-(Aminocarbonyl)cyclopentyl]-2-chlorobenzamide

https://huagongshe.com/reaction/1890704

반응식

참여 물질

역할이름HCID투입량
반응물TriethylamineHCID 8471—
반응물2-Chlorobenzoyl chlorideHCID 69110—
반응물1-Aminocyclopentane-1-carboxamide hydrochlorideHCID 54593188—
용매DichloromethaneHCID 6344—
생성물N-[1-(Aminocarbonyl)cyclopentyl]-2-chlorobenzamideHCID 58550576—

반응 단계

To a stirred solution of 1-aminocyclopentanecarboxamide hydrochloride (0.46 g, 2.79 mmol) in DCM (4 mL), cooled to 0° C., were added 2-chlorobenzoyl chloride (0.73 g, 4.19 mmol) and triethylamine (0.97 mL, 6.99 mmol). After stirring for 3 h, the precipitate in the reaction mixture was filtered to give the title compound.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08507477B2
출처 데이터셋uspto-grants-2013_08
ORD IDord-05604bc730ba4c5c973450cc98dcfd6d
출처 메모uspto-grants-2013_08