Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → N-[1-(Aminocarbonyl)cyclopentyl]-2-chlorobenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 2-Chlorobenzoyl chloride | HCID 69110 | — |
| 반응물 | 1-Aminocyclopentane-1-carboxamide hydrochloride | HCID 54593188 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | N-[1-(Aminocarbonyl)cyclopentyl]-2-chlorobenzamide | HCID 58550576 | — |
반응 단계
To a stirred solution of 1-aminocyclopentanecarboxamide hydrochloride (0.46 g, 2.79 mmol) in DCM (4 mL), cooled to 0° C., were added 2-chlorobenzoyl chloride (0.73 g, 4.19 mmol) and triethylamine (0.97 mL, 6.99 mmol). After stirring for 3 h, the precipitate in the reaction mixture was filtered to give the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08507477B2 |
| 출처 데이터셋 | uspto-grants-2013_08 |
| ORD ID | ord-05604bc730ba4c5c973450cc98dcfd6d |
| 출처 메모 | uspto-grants-2013_08 |