Hydrazine → 2-Hydrazinyl-4,8-dimethylquinoline

반응식

Cl[C:2]1[CH:11]=[C:10]([CH3:12])[C:9]2[C:4](=[C:5]([CH3:13])[CH:6]=[CH:7][CH:8]=2)[N:3]=1.[NH2:14][NH2:15]>>[NH:14]([C:2]1[CH:11]=[C:10]([CH3:12])[C:9]2[C:4](=[C:5]([CH3:13])[CH:6]=[CH:7][CH:8]=2)[N:3]=1)[NH2:15]

참가 물질

반응물 2

HCID 9321Hydrazine

HCID 2691612-Chloro-4,8-dimethylquinoline

생성물 1

HCID 36843162-Hydrazinyl-4,8-dimethylquinoline

실험 절차

A solution of 2-chloro-4,8-dimethylquinoline (1.00 g, 5.2 mmoles) in NH2NH2 was reacted as outlined in Scheme 1 above to give the desired title compound which was used in the next step without further purification.

출처 및 근거

ORD 기록: ord-6e7151b8bb97483b9a7a27f298eca9e7
출처 데이터셋: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08507682B2

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