p-Bromochlorobenzene → 8-(4-Chlorophenyl)-1,4-dioxaspiro[4.5]decan-8-ol

반응식

Br[C:2]1[CH:7]=[CH:6][C:5]([Cl:8])=[CH:4][CH:3]=1.[O:9]1[C:13]2([CH2:18][CH2:17][C:16](=[O:19])[CH2:15][CH2:14]2)[O:12][CH2:11][CH2:10]1>>[Cl:8][C:5]1[CH:6]=[CH:7][C:2]([C:16]2([OH:19])[CH2:17][CH2:18][C:13]3([O:12][CH2:11][CH2:10][O:9]3)[CH2:14][CH2:15]2)=[CH:3][CH:4]=1

참가 물질

반응물 2

HCID 7806p-Bromochlorobenzene

HCID 5674151,4-Dioxaspiro[4.5]decan-8-one

생성물 1

HCID 146178778-(4-Chlorophenyl)-1,4-dioxaspiro[4.5]decan-8-ol

실험 절차

The title compound was prepared as a white solid from 4-bromochlorobenzene (Aldrich) and 1,4-dioxa-spiro[4.5]decan-8-one using the procedure described in Step A of Example 1.

출처 및 근거

ORD 기록: ord-b424cd74c05946f2bae59fec916c0ad2
출처 데이터셋: uspto-grants-2013_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08513229B2

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