Cyclopropanol → Cyclopropylsulfamate

HRID 1893617노트

반응식

HRID 1893617 반응식
[C:1]1([O:7][S:8](=[O:11])(=[O:10])[NH2:9])[CH:6]=[CH:5]C=CC=1.[CH:12]1(O)[CH2:14][CH2:13]1>>[CH:12]1([NH:9][S:8](=[O:11])(=[O:10])[O-:7])[CH2:14][CH2:13]1.[CH:1]1([O:7][S:8](=[O:11])(=[O:10])[NH2:9])[CH2:5][CH2:6]1

참가 물질

4

반응물 2

HCID 123361CyclopropanolHCID 11030308Phenylsulfamate

생성물 2

HCID 21801555CyclopropylsulfamateHCID 57785190Cyclopropyl sulfamate

실험 절차

Cyclopropylsulfamate was synthesized according to the method presented in the synthesis of sulfamic acid phenyl ester in Example 1 with the exception of utilizing cyclopropanol (synthesized by methods reported in JOC 1980, 45, 4129-35) to obtain sulfamic acid cyclopropyl ester.

출처 및 근거

ORD 기록
ord-f0dba5a8226f48ceb0536a19d496f4b1
출처 데이터셋
uspto-grants-2013_08
특허 번호
US08513186B2

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