Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 6-Fluoro-2-naphthoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 6-Fluoro-2-naphthoic acid | HCID 2782788 | — |
| 생성물 | 6-Fluoro-2-naphthoyl chloride | HCID 86674834 | — |
반응 단계
6-fluoro-2-naphthoic acid (2 g, 10.52 mmol) was stirred in thionyl chloride (21.03 ml) at 80° C. for 4 h in pressure vessel. The mixture was cooled and concentrated. The acid chloride was dried and used as is for next step.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08519134B2 |
| 출처 데이터셋 | uspto-grants-2013_08 |
| ORD ID | ord-9bce67345cf24d389ebf4192955b9154 |
| 출처 메모 | uspto-grants-2013_08 |