Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thiophosgene → 2-Chloro-4-methylphenyl isothiocyanate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thiophosgene | HCID 10040 | — |
| 반응물 | 2-Chloro-p-toluidine | HCID 12007 | — |
| 반응물 | Diisopropylethylamine | HCID 81531 | — |
| 생성물 | 2-Chloro-4-methylphenyl isothiocyanate | HCID 143529 | 58.3% |
반응 단계
The title compound was prepared following the procedure described for intermediate-2 using 2-chloro-4-methyl aniline (2.0 g, 14.00 mmol), thiophosgene (1.62 g, 14.00 mmol) and N-ethyl di-isopropyl amine (3.63 g, 28.00 mmol) to afford 1.5 g of the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08519149B2 |
| 출처 데이터셋 | uspto-grants-2013_08 |
| ORD ID | ord-3b59b75f740b42dfa65e357b2132c9af |
| 출처 메모 | uspto-grants-2013_08 |