Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Iodopropane → N6-Methyl-N11-propyl-6,11-dihydro-5H-pyrido(2,3-b)(1,5)benzodiazepin-5-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Iodopropane | HCID 33643 | — |
| 반응물 | 5H-Pyrido(2,3-b)(1,5)benzodiazepin-5-one, 6,11-dihydro-6-methyl- | HCID 453245 | — |
| 생성물 | N6-Methyl-N11-propyl-6,11-dihydro-5H-pyrido(2,3-b)(1,5)benzodiazepin-5-one | HCID 453255 | 36% |
반응 단계
Using a procedure analogous to that described in Example 2, the product 6,11-dihydro-6-methyl-11-propyl-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one, m.p. 96°-98° C. (recrystal from petroleum ether) was prepared from 6,11-dihydro-6-methyl-5H-pyrido[2,3-b][1,5]benzodiazepin-5-one and 1-iodopropane. The yield was 36% of theory.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05571809 |
| 출처 데이터셋 | uspto-grants-1996_11 |
| ORD ID | ord-567270beae7d40ada4675bf13c175bea |
| 출처 메모 | uspto-grants-1996_11 |