Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1900719생성일: 2026년 10월 26일
2-Methanesulfonyloxymethyl-5-methyl-2,3,6,7-tetrahydrofuro[2,3-f]quinoline-7-one → 2-Iodomethyl-5-methyl-2,3,6,7-tetrahydrofuro-[2,3-f]quinoline-7-one
https://huagongshe.com/reaction/1900719
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Methanesulfonyloxymethyl-5-methyl-2,3,6,7-tetrahydrofuro[2,3-f]quinoline-7-one | HCID 23369644 | — |
| 반응물 | Sodium Iodate | HCID 23675764 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 2-Iodomethyl-5-methyl-2,3,6,7-tetrahydrofuro-[2,3-f]quinoline-7-one | HCID 23369711 | — |
반응 단계
To a solution of 2-methanesulfonyloxymethyl-5-methyl -2,3,6,7-tetrahydrofuro[2,3-f]quinoline-7-one (931 mg) in dimethylformamide (20 ml), sodium iodate (4.5 g) was added, and the mixture was stirred at 100° C. for 2 hours. After completion of the reaction, the solvent was distilled off, and the residue was purified by silica gel column chromatography (eluent: chloroform) to obtain 1 g (assayed quantitatively) of the target compound as a light yellow powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US05576324 |
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| 출처 데이터셋 | uspto-grants-1996_11 |
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| ORD ID | ord-070d70ff3d7840d5bf4cd059e38e424e |
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| 출처 메모 | uspto-grants-1996_11 |
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