Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-Methylheptylamine → 1-(4-Fluoro-2-nitrophenyl)-3-heptyl-3-methylurea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-Methylheptylamine | HCID 93190 | — |
| 반응물 | Phenyl 4-fluoro-2-nitrophenylcarbamate | HCID 23370075 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | 1-(4-Fluoro-2-nitrophenyl)-3-heptyl-3-methylurea | HCID 23370111 | — |
반응 단계
Phenyl 4-fluoro-2-nitrophenylcarbamate (0.70 g) and N-methylheptylamine (0.33 g) were dissolved in xylene (5 ml) and the solution was heated under reflux for 2 hrs. The solvent was distilled off and the residue was purified by a silica gel column chromatography (hexane:ethyl acetate=3:1) to give 1-(4-fluoro-2-nitrophenyl)-3-heptyl-3-methylurea as an oily product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05576335 |
| 출처 데이터셋 | uspto-grants-1996_11 |
| ORD ID | ord-0ed557f86cb647dda8e553acb0bf24a6 |
| 출처 메모 | uspto-grants-1996_11 |