Hydrazine → 1-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Carbazate

HRID 1902138노트

반응식

HRID 1902138 반응식
Cl[C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)=[O:3].[NH2:17][NH2:18]>CO>[C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)(=[O:3])[NH:17][NH2:18]

참가 물질

4

반응물 2

HCID 9321HydrazineHCID 540353651-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Cloroformate

생성물 1

HCID 536527591-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Carbazate

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

The title compound is prepared by reacting the compound of Example 27 (1 mole) with hydrazine (1.1 mole), employing methanol as the solvent.

출처 및 근거

ORD 기록
ord-763bc18c75244f2a82aa52d5e9a26908
출처 데이터셋
uspto-grants-1996_11
특허 번호
US05578731

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