HCID 15575166, 화합물 → HCID 15575176, 화합물
반응식
[CH3:1][C:2]1[C:7]2[S:8][C:9]3([C:15](=[O:16])[C:6]=2[CH:5]=[CH:4][CH:3]=1)[CH2:13][CH2:12]OC3=O>C(O)C.O>[CH3:1][C:2]1[C:7]2[S:8][C:9]3([C:15](=[O:16])[C:6]=2[CH:5]=[CH:4][CH:3]=1)[CH2:13][CH2:12]3참가 물질
3
실험 절차
7-Methylspiro[benzo[b]thiophene-2(3H),1'-cyclopropan]-3-one was prepared by a similar procedure to that of Example 8 except for the use of 7-methyl-4',5'-dihydrospiro[benzo[b]thiophene-2(3H),3'(2'H)-furan]-3,2'-dione obtained in Reference Example 11. Pale yellow needles [from C2H5OH--H2O (1:1)], mp 74°-75° C. Anal. Calcd. for C11H10OS: C, 69.44; H, 5.30. Found: C, 69.32; H, 5.07.
후처리
- customobtained in Reference Example 11
출처 및 근거
- ORD 기록
- ord-f2425512e5b34a63b8f9ece7d8dc3cee
- 출처 데이터셋
- uspto-grants-1982_12
- 특허 번호
- US04362740
반응 노트
불러오는 중…