Diethyl Malonate → HCID 12509451, 화합물

반응식

[Cl:1][CH2:2][C:3](=O)[CH:4]=[CH:5][Cl:6].[C:8]([O:16][CH2:17][CH3:18])(=[O:15])[CH2:9][C:10]([O:12][CH2:13][CH3:14])=[O:11]>>[C:8]([C:9](=[C:3]([CH2:2][Cl:1])/[CH:4]=[CH:5]/[Cl:6])[C:10]([O:12][CH2:13][CH3:14])=[O:11])([O:16][CH2:17][CH3:18])=[O:15]

참가 물질

반응물 2

HCID 7761Diethyl Malonate

HCID 53421801HCID 53421801, 화합물

생성물 1

HCID 12509451HCID 12509451, 화합물수율 76.9%

실험 절차

1,4-Dichloro-3-buten-2-one (0.0556 kg, 0.4 mole) and diethyl malonate (0.064 kg, 0.4 mole) were condensed under identical conditions to those described in Example 1(b) to give the title compound 0.0865 kg (77%; purity, g.l.c., 87.85%).

후처리

customcondensed under identical conditions to

출처 및 근거

ORD 기록: ord-b30f4203052a4456ba4fa70c3e9da280
출처 데이터셋: uspto-grants-1982_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04362880

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