참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phenol | HCID 996 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 2,3,4,5-Tetrachloronitrobenzene | HCID 13428 | — |
| 용매 | Sodium Hydroxide | HCID 14798 | — |
| 생성물 | 2,6-Dichloro-4-nitro-1,3-diphenoxy-benzene | HCID 12881148 | — |
반응 단계
A mixture of 52.4 gm of 2,3,4,5-tetrachloro-1-nitro-benzene, 122 gm of phenol and 60 gm of potassium carbonate was heated for 11/2 hours at 160° C. Thereafter, the still hot reaction mixture was stirred into 1.2 liters of 2 N sodium hydroxide, and the precipitated product was collected by suction filtration and recrystallized from 300 ml of ethyl acetate. 70.5 gm (93.8% of theory) of the title compound, m.p. 164° C., were obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04364875 |
|---|
| 출처 데이터셋 | uspto-grants-1982_12 |
|---|
| ORD ID | ord-508ef23d214848a7954823fff63c343f |
|---|
| 출처 메모 | uspto-grants-1982_12 |
|---|
