참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Fluorosulfuric acid, ethyl ester | HCID 67791 | — |
| 반응물 | 7-Methoxybenzotelluropyrone | HCID 88739849 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 4-Ethoxy-7-methoxybenzotelluropyrone Fluorosulfonate | HCID 88749835 | 87% |
반응 단계
Five g of 7-methoxybenzotelluropyrone was added to 20 ml of freshly distilled ethyl fluorosulfonate. The resulting mixture was stirred under nitrogen at 60° C. for 10 minutes. Two hundred ml of ether was added precipitating a red solid. The product was collected by filtration and recrystallized from acetonitrile to give 6.0 g (87%) of a red solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04365017 |
|---|
| 출처 데이터셋 | uspto-grants-1982_12 |
|---|
| ORD ID | ord-43b52567e692450fa38bf11e977429f0 |
|---|
| 출처 메모 | uspto-grants-1982_12 |
|---|
