Toluene → 4-(2',4',6'-Trifluorophenyl)-carbethoxysemicarbazide
반응식
C1(C)C=CC=CC=1.[F:8][C:9]1[CH:15]=[C:14]([F:16])[CH:13]=[C:12]([F:17])[C:10]=1[NH2:11].[C:18]([NH:23][NH:24][C:25](Cl)=[O:26])([O:20][CH2:21][CH3:22])=[O:19]>C(OCC)(=O)C.C1(C)C=CC=CC=1>[F:8][C:9]1[CH:15]=[C:14]([F:16])[CH:13]=[C:12]([F:17])[C:10]=1[NH:11][C:25](=[O:26])[NH:24][NH:23][C:18]([O:20][CH2:21][CH3:22])=[O:19]참가 물질
5
실험 절차
A toluene solution of 2,4,6-trifluoroaniline is reacted with 2-carbethoxyhydrazinecarbonyl chloride as described above in Example 1b, mp 177°-178° (ethyl acetate/toluene).
출처 및 근거
- ORD 기록
- ord-3574e8679a7842c585f3b7dcf2e120cf
- 출처 데이터셋
- uspto-grants-1982_12
- 특허 번호
- US04366320
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