Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 1-Ethyl-3-phenylurea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Aniline | HCID 6115 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | HCID 178464749 | HCID 178464749 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 1-Ethyl-3-phenylurea | HCID 12115 | 79% |
반응 단계
5.08 g ethylcarbamoyl-benzoic acid sulfimide was reacted with 1.86 g aniline and 2.8 ml triethylamine in 20 ml of a 1:1 mixture of water and acetone, as described in example 1. 2.59 g 1-phenyl-3-ethylurea was obtained, melting at 99°-100° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04435567 |
| 출처 데이터셋 | uspto-grants-1984_03 |
| ORD ID | ord-35440c9b9e2543be8db34146e9f698d2 |
| 출처 메모 | uspto-grants-1984_03 |