Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-(3-Phenyl-1-propenyl)aniline → 3-(3-Phenylpropyl)aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-(3-Phenyl-1-propenyl)aniline | HCID 54042989 | — |
| 촉매 | HCID 178418390 | HCID 178418390 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3-(3-Phenylpropyl)aniline | HCID 427307 | 92% |
반응 단계
A solution of 3-(3-phenyl-1-propenyl)aniline (3.6 g) in 50 ml of ethanol was subjected to catalytic reduction using 1 g of 10% palladium-carbon. After removal of the catalyst by filtration, the solvent was removed under reduced pressure. The residue was distilled under reduced pressure to give 3.3 g of 3-(3-phenylpropyl)aniline (yield, 92%). B.P. 122°-126° C./0.08 mmHg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04437880 |
| 출처 데이터셋 | uspto-grants-1984_03 |
| ORD ID | ord-14973120f72e4eb5953e84b360c0baf4 |
| 출처 메모 | uspto-grants-1984_03 |