HCID 54049138, 화합물 → HCID 13316973, 화합물
반응식
[Br:1][CH2:2][CH2:3][CH:4]=[CH:5][CH2:6][CH2:7][C:8]1[CH:15]=[CH:14][C:11]([C:12]#[N:13])=[CH:10][CH:9]=1>C(O)C.[Pt]=O>[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]1[CH:15]=[CH:14][C:11]([C:12]#[N:13])=[CH:10][CH:9]=1참가 물질
4
실험 절차
A solution of 10.5 g of 4-(6-bromohex-3-enyl)benzonitrile in 200 ml of absolute ethanol was hydrogenated in the presence of 0.25 g of platinum oxide catalyst. Isolation of the product afforded 10.4 g of 4-(6-bromohexyl)benzonitrile as a yellow oil which was distilled at 168°-170° C.(0.01 mm) to produce the compound as a colorless oil which solidfied upon cooling.
출처 및 근거
- ORD 기록
- ord-650cfc9ff51a4789b5f4463826c00b89
- 출처 데이터셋
- uspto-grants-1989_06
- 특허 번호
- US04843087
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