반응식
O[CH2:2][NH:3][C:4](=[O:11])[C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1.S(=O)(=O)(O)O.[Cl:17][C:18]1[CH:23]=[CH:22][C:21]([C:24]2[N:25]=[C:26]3[CH:31]=[CH:30][C:29]([CH3:32])=[CH:28][N:27]3[CH:33]=2)=[CH:20][CH:19]=1>C(O)(=O)C>[Cl:17][C:18]1[CH:19]=[CH:20][C:21]([C:24]2[N:25]=[C:26]3[CH:31]=[CH:30][C:29]([CH3:32])=[CH:28][N:27]3[C:33]=2[CH2:2][NH:3][C:4](=[O:11])[C:5]2[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=2)=[CH:22][CH:23]=1참가 물질
5
반응 조건
- 온도
- 50 °C
실험 절차
To a solution of 4.54 g (0.03 mol) of N-(hydroxymethyl)benzamide in 50 ml of glacial acetic acid, 2 g of concentrated sulphuric acid are added, and then, after 15 minutes' heating at 50° C., 4.8 g (0.02 mol) of 2-(4-chlorophenyl)-6-methylimidazo[1,2-a]pyridine are added.
출처 및 근거
- ORD 기록
- ord-f09ddaa63a2d4d9f960d9774a8536c03
- 출처 데이터셋
- uspto-grants-1987_03
- 특허 번호
- US04650796
연결된 노트
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